Synthesis and structure of the bilayer hydrate Na0.3NiO 2·1.3D2O

Sangmoon Park, Yongjae Lee, Margaret Elcombe, Thomas Vogt

Research output: Contribution to journalArticlepeer-review

17 Citations (Scopus)


The metal oxide bilayer deuterate (hydrate) Na0.3NiO 2·1.3D2O (Na0.3NiO2·1. 3H2O) were prepared from NaxNiO2 by extracting Na+ cations and simultaneously intercalating fully and nondeuterated water. High-resolution neutron powder diffraction, thermogravimetric analysis, and inductively coupled plasma atomic emission spectroscopy were used to show that a Na0.3(D2O)1.3 network separates layers of edge-sharing NiO6 octahedra.

Original languageEnglish
Pages (from-to)3490-3492
Number of pages3
JournalInorganic Chemistry
Issue number9
Publication statusPublished - 2006 May 1

All Science Journal Classification (ASJC) codes

  • Physical and Theoretical Chemistry
  • Inorganic Chemistry


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