Direct synthesis of acyl azides from carboxylic acids by the combination of trichloroacetonitrile, triphenylphosphine and sodium azide

Joong Gon Kim; Doo Ok Jang

doi:10.1055/s-2008-1077979

Direct synthesis of acyl azides from carboxylic acids by the combination of trichloroacetonitrile, triphenylphosphine and sodium azide

Joong Gon Kim, Doo Ok Jang

Chemistry and Medical Chemistry

Research output: Contribution to journal › Article › peer-review

20 Citations (Scopus)

Abstract

Various carboxylic acids were converted into acyl azides in excellent yields by treating with trichloroacetonitrile, triphenylphosphine and sodium azide at room temperature. The reaction was applicable to the preparation of dipeptide without rearrangement.

Original language	English
Pages (from-to)	2072-2074
Number of pages	3
Journal	Synlett
Issue number	13
DOIs	https://doi.org/10.1055/s-2008-1077979
Publication status	Published - 2008 Aug 1

All Science Journal Classification (ASJC) codes

Organic Chemistry

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title = "Direct synthesis of acyl azides from carboxylic acids by the combination of trichloroacetonitrile, triphenylphosphine and sodium azide",

abstract = "Various carboxylic acids were converted into acyl azides in excellent yields by treating with trichloroacetonitrile, triphenylphosphine and sodium azide at room temperature. The reaction was applicable to the preparation of dipeptide without rearrangement.",

author = "Kim, {Joong Gon} and Jang, {Doo Ok}",

year = "2008",

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doi = "10.1055/s-2008-1077979",

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AU - Kim, Joong Gon

AU - Jang, Doo Ok

PY - 2008/8/1

Y1 - 2008/8/1

N2 - Various carboxylic acids were converted into acyl azides in excellent yields by treating with trichloroacetonitrile, triphenylphosphine and sodium azide at room temperature. The reaction was applicable to the preparation of dipeptide without rearrangement.

AB - Various carboxylic acids were converted into acyl azides in excellent yields by treating with trichloroacetonitrile, triphenylphosphine and sodium azide at room temperature. The reaction was applicable to the preparation of dipeptide without rearrangement.

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JF - Synlett

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ER -

Direct synthesis of acyl azides from carboxylic acids by the combination of trichloroacetonitrile, triphenylphosphine and sodium azide

Abstract

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